Online Library TheLib.net » Advances in X-Ray Analysis: Volume 27
Content:
Front Matter....Pages i-xviii
Establishment of the J. D. Hanawalt Award for Excellence in Powder Diffraction and its First Presentation to Ludo K. Frevel....Pages 1-2
J. D. Hanawalt Powder Diffraction Award Lecture....Pages 3-18
Presentation of the J. D. Hanawalt Award....Pages 19-20
Computer Techniques for Faster X-Ray Diffraction Phase Identification....Pages 21-26
Fuzzy Sets and Inverted Search — Two Concepts for Compound Identification in Spectra....Pages 27-34
PDF Search and Match Algorithms for the Cyber 205 Vector Processor....Pages 35-36
A Method of Background Subtraction for the Analysis of Broadened Profiles....Pages 37-44
A Combined Derivative Method for Peak Search Analysis....Pages 45-52
Experimental Study of Precise Peak Determination in X-Ray Powder Diffraction....Pages 53-60
Evaluation of Existing X-Ray Powder Diffraction Standards for Phosphate Minerals....Pages 61-66
Data Sets for Evaluation of Powder Diffraction Search/Match Algorithms....Pages 67-74
Computer Simulation of Powder Patterns....Pages 75-80
A Useful Guide for X-Ray Stress Evaluation (XSE)....Pages 81-99
Stress Evaluation on Materials Having Non-Linear Lattice Strain Distributions....Pages 101-120
X-Ray Multiaxial Stress Analysis Taking Account of Stress Gradient....Pages 121-128
Determining Stresses in the Presence of Nonlinearities in Interplay Spacing vs. Sin2?....Pages 129-148
On the Use of Synchrotron Radiation for the Study of the Mechanical Behaviour of Materials....Pages 149-158
The Measurement of Elastic Constants for the Determination of Stresses by X-Rays....Pages 159-170
X-Ray Strain Measurements in IV–VI-Semiconductor Superlattices at Low Temperature....Pages 171-178
Recent Applications of XSA in Heat Treatment and Fatigue of Steels....Pages 179-190
Stress Measurement at Fatigue Crack Tip Using PSPC....Pages 191-196
Direct X-Ray Measurement of Residual Strains in Textured Steel....Pages 197-206
A Study of Plastic Flow and Residual Stress Distribution Caused by Rolling Contact....Pages 207-212
X-Ray Fractography on Stress Corrosion Cracking of High Strength Steel....Pages 213-220
Determination of Residual Stresses in Transformation-Toughened Ceramics....Pages 221-228
Small Area X-Ray Diffraction Techniques; Applications of the Micro-Diffractometer to Phase Identification and Strain Determination....Pages 229-238
Residual Stress Relaxation in Cemented Carbide Composites Studied Using the Argonne Intense Pulsed Neutron Source....Pages 239-249
Stress Determination in an Adhesive Bonded Joint By X-Ray Diffraction....Pages 251-260
Evaluation of Straight and Curved Braun Position-Sensitive Proportional Counters on a Huber-Guinier X-Ray Diffraction System....Pages 261-266
A New in Situ, Automatic, Strain-Measuring X-Ray Diffraction Apparatus with PSD....Pages 267-272
A Miniature Instrument for Residual Stress Measurement....Pages 273-283
A Low-High Temperature Camera for in-situ X-Ray Diffraction Studies of Catalysts....Pages 285-291
A Low Cost Rejuvenation of Old G.E. and Picker X-Ray Generators....Pages 293-297
An Inexpensive In-House EXAFS Spectrometer....Pages 299-305
Suppression of X-Ray Fluorescence Background in X-Ray Powder Diffraction by a Mercuric Iodide Spectrometer....Pages 307-316
Computer-Assisted Alignment of a Guinier X-Ray Powder Diffraction System....Pages 317-330
Energy Dispersive Diffraction in a Diamond Anvil High Pressure Cell using Synchrotron and Conventional X-Radiation....Pages 331-337
Reference Intensity Quantitative Analysis using Thin-Layer Aerosol Samples....Pages 339-348
Quantitative Analysis: A Comparative Study using Mo and Cu Radiation on Coal Related Minerals and Fly Ash....Pages 349-354
Multiphase Quantitative Analysis of Colorado Oil Shales Involving Overlap of the Diffraction Peaks....Pages 355-362
Evidence for Stacking Faults in Multiaxial Strained Alpha-Brass....Pages 363-368
Line Broadening Studies on Highly Defective Al2O3 Produced by High Pressure Shock Loading....Pages 369-378
Line Broadening Studies on Highly Defective TiO2 Produced by High Pressure Shock Loading....Pages 379-388
Examination of the Reaction Kinetics at Solder/Metal Interfaces via High Temperature X-Ray Diffraction....Pages 389-395
High Temperature Guinier X-Ray Diffractometry for Thermal Expansion Measurements in the Hexagonal Form of Cordierite (2MgO·2A12O3·5SiO2)....Pages 397-404
Continuing Development of Mercuric Iodide X-Ray Spectrometry....Pages 405-414
X-Ray Tube Improvements for Better Performance in an Energy-Dispersive X-Ray Spectrometer System....Pages 415-422
Comparison of Experimental and Theoretical Intensities for a New X-Ray Tube for Light Element Analysis....Pages 423-426
Using a Microcomputer-Controlled Robot Arm as a General Purpose Sample Changer....Pages 427-432
Lama III — A Computer Program for Quantitative XRFA of Bulk Specimens and Thin Film Layers....Pages 433-440
An Empirical Background Calculation Method for Multi-Channel X-Ray Spectrometers....Pages 441-448
Comparison of X-ray Backscatter Parameters for Complete Sample Matrix Definition....Pages 449-457
Investigation of Obsidian by Radioisotope X-ray Fluorescence....Pages 459-466
A Comparison of Trace Metal Determinations in Contaminated Soils by XRF and ICAP Spectroscopies....Pages 467-473
Determination of Barium and Selected Rare-Earth Elements in Geological Materials Employing a HpGe Detector by Radioisotope Excited X-Ray Fluorescence....Pages 475-480
A Versatile XRF Analytical System for Geochemical Exploration and Other Applications....Pages 481-486
XRF Analysis of Low Level Cation Concentration of Sodium Silicate Solutions....Pages 487-490
A Rapid, Low Cost, Manual Fusion Sample Preparation Technique for Quantitative X-Ray Fluorescence Analysis....Pages 491-496
Quantitative X-Ray Fluorescence Analysis for Fly Ash Samples....Pages 497-504
Polarization of X-Rays by Scattering from the Interior of a Cylinder....Pages 505-511
Polarization of X-Rays by Scattering from the Interior of a Cylinder....Pages 513-517
Application of a Polarized X-Ray Spectrometer for Analysis of Ash from a Refuse-Fired Steam Generating Facility....Pages 519-526
Applications of Room Temperature Energy Dispersive X-Ray Spectrometry Using a Mercuric Iodide Detector....Pages 527-537
Wall Effect and Detection Limit of the Proportional Counter Spectrometer....Pages 539-546
Determination of Oxygen and Nitrogen in Various Materials by X-Ray Fluorescence Spectrometry....Pages 547-556
Trace Element Analysis by Synchrotron Radiation Excited XRF....Pages 557-562
X-Ray Fluorescence Spectrometric Analysis of Uncontaminated and Contaminated Tropical Plant Materials for Traces of Heavy Metals....Pages 563-570
Back Matter....Pages 571-579



Content:
Front Matter....Pages i-xviii
Establishment of the J. D. Hanawalt Award for Excellence in Powder Diffraction and its First Presentation to Ludo K. Frevel....Pages 1-2
J. D. Hanawalt Powder Diffraction Award Lecture....Pages 3-18
Presentation of the J. D. Hanawalt Award....Pages 19-20
Computer Techniques for Faster X-Ray Diffraction Phase Identification....Pages 21-26
Fuzzy Sets and Inverted Search — Two Concepts for Compound Identification in Spectra....Pages 27-34
PDF Search and Match Algorithms for the Cyber 205 Vector Processor....Pages 35-36
A Method of Background Subtraction for the Analysis of Broadened Profiles....Pages 37-44
A Combined Derivative Method for Peak Search Analysis....Pages 45-52
Experimental Study of Precise Peak Determination in X-Ray Powder Diffraction....Pages 53-60
Evaluation of Existing X-Ray Powder Diffraction Standards for Phosphate Minerals....Pages 61-66
Data Sets for Evaluation of Powder Diffraction Search/Match Algorithms....Pages 67-74
Computer Simulation of Powder Patterns....Pages 75-80
A Useful Guide for X-Ray Stress Evaluation (XSE)....Pages 81-99
Stress Evaluation on Materials Having Non-Linear Lattice Strain Distributions....Pages 101-120
X-Ray Multiaxial Stress Analysis Taking Account of Stress Gradient....Pages 121-128
Determining Stresses in the Presence of Nonlinearities in Interplay Spacing vs. Sin2?....Pages 129-148
On the Use of Synchrotron Radiation for the Study of the Mechanical Behaviour of Materials....Pages 149-158
The Measurement of Elastic Constants for the Determination of Stresses by X-Rays....Pages 159-170
X-Ray Strain Measurements in IV–VI-Semiconductor Superlattices at Low Temperature....Pages 171-178
Recent Applications of XSA in Heat Treatment and Fatigue of Steels....Pages 179-190
Stress Measurement at Fatigue Crack Tip Using PSPC....Pages 191-196
Direct X-Ray Measurement of Residual Strains in Textured Steel....Pages 197-206
A Study of Plastic Flow and Residual Stress Distribution Caused by Rolling Contact....Pages 207-212
X-Ray Fractography on Stress Corrosion Cracking of High Strength Steel....Pages 213-220
Determination of Residual Stresses in Transformation-Toughened Ceramics....Pages 221-228
Small Area X-Ray Diffraction Techniques; Applications of the Micro-Diffractometer to Phase Identification and Strain Determination....Pages 229-238
Residual Stress Relaxation in Cemented Carbide Composites Studied Using the Argonne Intense Pulsed Neutron Source....Pages 239-249
Stress Determination in an Adhesive Bonded Joint By X-Ray Diffraction....Pages 251-260
Evaluation of Straight and Curved Braun Position-Sensitive Proportional Counters on a Huber-Guinier X-Ray Diffraction System....Pages 261-266
A New in Situ, Automatic, Strain-Measuring X-Ray Diffraction Apparatus with PSD....Pages 267-272
A Miniature Instrument for Residual Stress Measurement....Pages 273-283
A Low-High Temperature Camera for in-situ X-Ray Diffraction Studies of Catalysts....Pages 285-291
A Low Cost Rejuvenation of Old G.E. and Picker X-Ray Generators....Pages 293-297
An Inexpensive In-House EXAFS Spectrometer....Pages 299-305
Suppression of X-Ray Fluorescence Background in X-Ray Powder Diffraction by a Mercuric Iodide Spectrometer....Pages 307-316
Computer-Assisted Alignment of a Guinier X-Ray Powder Diffraction System....Pages 317-330
Energy Dispersive Diffraction in a Diamond Anvil High Pressure Cell using Synchrotron and Conventional X-Radiation....Pages 331-337
Reference Intensity Quantitative Analysis using Thin-Layer Aerosol Samples....Pages 339-348
Quantitative Analysis: A Comparative Study using Mo and Cu Radiation on Coal Related Minerals and Fly Ash....Pages 349-354
Multiphase Quantitative Analysis of Colorado Oil Shales Involving Overlap of the Diffraction Peaks....Pages 355-362
Evidence for Stacking Faults in Multiaxial Strained Alpha-Brass....Pages 363-368
Line Broadening Studies on Highly Defective Al2O3 Produced by High Pressure Shock Loading....Pages 369-378
Line Broadening Studies on Highly Defective TiO2 Produced by High Pressure Shock Loading....Pages 379-388
Examination of the Reaction Kinetics at Solder/Metal Interfaces via High Temperature X-Ray Diffraction....Pages 389-395
High Temperature Guinier X-Ray Diffractometry for Thermal Expansion Measurements in the Hexagonal Form of Cordierite (2MgO·2A12O3·5SiO2)....Pages 397-404
Continuing Development of Mercuric Iodide X-Ray Spectrometry....Pages 405-414
X-Ray Tube Improvements for Better Performance in an Energy-Dispersive X-Ray Spectrometer System....Pages 415-422
Comparison of Experimental and Theoretical Intensities for a New X-Ray Tube for Light Element Analysis....Pages 423-426
Using a Microcomputer-Controlled Robot Arm as a General Purpose Sample Changer....Pages 427-432
Lama III — A Computer Program for Quantitative XRFA of Bulk Specimens and Thin Film Layers....Pages 433-440
An Empirical Background Calculation Method for Multi-Channel X-Ray Spectrometers....Pages 441-448
Comparison of X-ray Backscatter Parameters for Complete Sample Matrix Definition....Pages 449-457
Investigation of Obsidian by Radioisotope X-ray Fluorescence....Pages 459-466
A Comparison of Trace Metal Determinations in Contaminated Soils by XRF and ICAP Spectroscopies....Pages 467-473
Determination of Barium and Selected Rare-Earth Elements in Geological Materials Employing a HpGe Detector by Radioisotope Excited X-Ray Fluorescence....Pages 475-480
A Versatile XRF Analytical System for Geochemical Exploration and Other Applications....Pages 481-486
XRF Analysis of Low Level Cation Concentration of Sodium Silicate Solutions....Pages 487-490
A Rapid, Low Cost, Manual Fusion Sample Preparation Technique for Quantitative X-Ray Fluorescence Analysis....Pages 491-496
Quantitative X-Ray Fluorescence Analysis for Fly Ash Samples....Pages 497-504
Polarization of X-Rays by Scattering from the Interior of a Cylinder....Pages 505-511
Polarization of X-Rays by Scattering from the Interior of a Cylinder....Pages 513-517
Application of a Polarized X-Ray Spectrometer for Analysis of Ash from a Refuse-Fired Steam Generating Facility....Pages 519-526
Applications of Room Temperature Energy Dispersive X-Ray Spectrometry Using a Mercuric Iodide Detector....Pages 527-537
Wall Effect and Detection Limit of the Proportional Counter Spectrometer....Pages 539-546
Determination of Oxygen and Nitrogen in Various Materials by X-Ray Fluorescence Spectrometry....Pages 547-556
Trace Element Analysis by Synchrotron Radiation Excited XRF....Pages 557-562
X-Ray Fluorescence Spectrometric Analysis of Uncontaminated and Contaminated Tropical Plant Materials for Traces of Heavy Metals....Pages 563-570
Back Matter....Pages 571-579
....
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